Crystal structure of 1-methyl-5-(4-(1-methyl-1H-tetrazol-5-ylthio) butylthio)-1H-tetrazole, C8H14N8S2

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In the title compound, C22H18N8 H2O, the dihedral angle between the tetrazole rings is 69.58 (1) while the terminal phenyl ring makes dihedral angles of 26.98 (8) and 39.75 (8) with the other benzene rings. The rings of the biphenyl unit subtend a dihedral angle of 55.23 (8) . In the crystal, the solvent water molecule is linked to the main molecule via an N—H O hydrogen bond. In addition, C—H ...

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In the title compound, C12H12N6S, the dihedral angles between the central pyrazole ring and the pendant triazole and benzene rings are 68.01 (4) and 59.83 (9)°, respectively. In the crystal, mol-ecules are linked by N-H⋯N and N-H⋯S hydrogen bonds, generating (10-1) sheets.

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The title compound, C(20)H(16)Cl(2)N(4)O, has two mol-ecules in the asymmetric unit. The two five-membered rings form a dihedral angle of 54.2 (3)° in one mol-ecule and 56.8 (3)° in the other independent mol-ecule. The amino group of the dihydro-pyrazolone unit of one mol-ecule acts as a hydrogen-bond donor to the carbonyl group of the dihydro-pyrazolone system of the other mol-ecule. The resul...

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ژورنال

عنوان ژورنال: Zeitschrift für Kristallographie - New Crystal Structures

سال: 2013

ISSN: 2197-4578,1433-7266

DOI: 10.1524/ncrs.2013.0007